Solid-State NMR Spectroscopy of Inorganic Materials

by John J. Fitzgerald

Overview

This book describes recent advances in solid-state NMR methods as applied to modern inorganic materials such as metal oxides, catalysts, zeolites, glasses, ceramics, semiconductors, ion conductors, super-conductors, and composites.

Product Details

ISBN-13:	9780841236028
Publisher:	American Chemical Society
Publication date:	01/28/1999
Series:	ACS Symposium Series , #717
Pages:	432
Product dimensions:	6.10(w) x 9.10(h) x 1.00(d)

Table of Contents

Preface
Introduction
1. Solid-State NMR Spectroscopy of Inorganic Materials: An Overview, John J. Fitzgerald and Susan M. DePaul
NMR of Metal Oxide Systems
2. Multiple-Quantum Magic-Angle Spinning NMR of Half-Integer Quadrupolar Nuclei, Ales Medek, Laura Marinelli, and Lucio Frydman
3. Oxygen Motion in Simple and Complex Oxides, Jeffrey A. Reimer and Stuart B. Adler
4. The Study of Fluoridated Hydroxyapatite by ³¹P-¹]9F Rotational-Echo, Double-Resonance NMR, Yong Pan
5. Solid-State ¹H, ¹]7O, and ²]7Al NMR Studies of the Surface Chemistry of Alumina Materials, John J. Fitzgerald
Solid-State NMR of Amorphous Glasses and Gels
6. An Overview of Solid-State NMR Correlation Experiments in Phosphate Glass Systems, R. M. Wenslow, K. Fiske, and K. T. Mueller
7. Borate Glass Structure Probed with Dynamic Angle Spinning NMR, J. W. Zwanziger, R. E. Youngman, and M. Braun
8. A ¹]7O Solid State NMR Study of the Lead Zirconium Titanate System (PBZr[xTi[1[-[xO[3), Walter G. Klemperer and David L. Richard
NMR Studies of Silica-Containing Materials
9. Multinuclear NMR Study of Host-Guest Interactions in Sodalites, G. Engelhardt
10. Investigation of the Host-Guest Structures of Molecular Sieves by One- and Two-Dimensional Solid-State NMR Techniques, C.A. Fyfe et al.
11. Double-Resonance and Two-Dimensional Silicon-29 NMR Spectroscopy of Minerals, Jay S. Shore et al.
12. Siloxane-Based Solid Networks, from Silicas to Silicones, Gary E. Maciel
NMR Studies of Inorganic Nitrogen-Containing Solids
13. Wide-Line ¹]4N NMR in Solids, James P. Yesinowski and Edward A. Hill
14. Solid-State NMR of Nitrides and Oxynitrides, M. E. Smith
Author Index
Subject Index

Editorial Reviews

"The collection of 14 papers, developed from a August 1996 symposium sponsored by the division of industrial and engineering chemistry of the ACS, summarizes recent developments in the use of solid-state nuclear magnetic resonance (NMR) to investigate inorganic materials. Four sections discuss NMR studies of metal oxide systems, amorphous glasses and gels, silica-containing materials, and inorganic nitrogen- containing solids. Among the topics are multiple-quantum magic-angle spinning NMR of half-integer quadrupolar nuclei, 2D heteronuclear correlation NMR experiments of phosphate glasses, the exploration of guest-host interactions in sodalites by multinuclear NMR, and NMR of nitride and oxynitride ceramic materials."—SciTech Book News

From the Publisher

The collection of 14 papers, developed from a August 1996 symposium sponsored by the division of industrial and engineering chemistry of the ACS, summarizes recent developments in the use of solid-state nuclear magnetic resonance (NMR) to investigate inorganic materials. Four sections discuss NMR studies of metal oxide systems, amorphous glasses and gels, silica-containing materials, and inorganic nitrogen- containing solids. Among the topics are multiple-quantum magic-angle spinning NMR of half-integer quadrupolar nuclei, 2D heteronuclear correlation NMR experiments of phosphate glasses, the exploration of guest-host interactions in sodalites by multinuclear NMR, and NMR of nitride and oxynitride ceramic materials. Distributed by Oxford University Press. Annotation c. Book News, Inc., Portland, OR (booknews.com)

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